NOTICES
Environmental Laboratory Accreditation Proficiency Test Study Requirements
[36 Pa.B. 1181] In accordance with 25 Pa. Code Chapter 252, Subchapter E (relating to proficiency test study requirements), the Department of Environmental Protection (Department) is providing the following tables which list the fields of accreditation for which proficiency test studies are available. To obtain or maintain a field of accreditation, the Department requires that an environmental laboratory successfully participate in proficiency test studies when available. The following tables contain fields of accreditation for which proficiency test studies are available for nonpotable water (NPW), drinking water and solid and chemical materials. Environmental laboratories seeking initial accreditation must successfully complete a proficiency test study within 12 months prior to applying for initial accreditation or during the approval process. Environmental laboratories seeking to maintain accreditation must successfully complete a proficiency test study for each field of accreditation at least once every 12 months. Additional information regarding the proficiency test study requirements is contained in 25 Pa. Code Chapter 252, Subchapter E.
Updates to the following lists will be published in the Pennsylvania Bulletin as revisions are made. Questions concerning this notice, including the lists of proficiency testing currently available, should be directed to Aaren Alger, Department of Environmental Protection, Bureau of Laboratories, (717) 346-8212, aaalger@state.pa.us.
KATHLEEN A. MCGINTY,
Secretary
Pennsylvania State (Chapter 252) Accreditation
Fields of Proficiency Testing
Nonpotable Water (NPW)
Effective January 28, 2006
Matrix Analyte Microbiology NPW Total Coliform, MF NPW Fecal Coliform, MF NPW Enterococci, MF NPW Total Coliform, MPN NPW Fecal Coliform, MPN NPW Enterococci, MPN Trace Metals NPW Aluminum NPW Antimony NPW Arsenic NPW Barium NPW Beryllium NPW Boron NPW Cadmium NPW Chromium, total NPW Chromium VI NPW Cobalt NPW Copper NPW Iron NPW Lead NPW Manganese NPW Mercury NPW Molybdenum NPW Nickel NPW Selenium NPW Silver NPW Strontium NPW Thallium NPW Tin NPW Titanium NPW Vanadium NPW Zinc Demands NPW 5-day BOD NPW Carbonaceous BOD NPW COD NPW TOC Minerals NPW Alkalinity, total (CaCO3) NPW Calcium NPW Chloride NPW Fluoride NPW Calcium hardness as CaCO3 NPW Hardness, total (CaCO3) NPW Magnesium NPW Potassium NPW Sodium NPW Spec. Cond. (25°C) NPW Sulfate NPW Sulfide NPW Total Dissolved Solids at 180°C NPW Total Solids Nutrients NPW Ammonia as N NPW Nitrate as N NPW Nitrate-nitrite as N NPW Nitrite as N NPW Orthophosphate as P NPW Total Kjeldahl-Nitrogen NPW Total Phosphorus Misc. Analytes NPW Non-Filterable Residue NPW Oil & Grease NPW Total Petroleum Hydrocarbons1 NPW pH NPW Total Cyanide NPW Total Phenolics (4AAP) NPW Total Residual Chlorine NPW Surfactants--MBAS Pesticides NPW Aldrin NPW alpha-BHC NPW beta-BHC NPW delta-BHC NPW gamma-BHC (Lindane) NPW alpha-Chlordane NPW gamma-Chlordane NPW Chlordane (total) NPW DDD (4,4) NPW DDE (4,4) NPW DDT (4,4) NPW Dieldrin NPW Endosulfan I NPW Endosulfan II NPW Endosulfan sulfate NPW Endrin NPW Endrin aldehyde NPW Heptachlor NPW Heptachlor Epoxide (beta) NPW Methoxychlor NPW Toxaphene Volatile Aromatics NPW Benzene NPW 1,2 Dichlorobenzene NPW 1,3 Dichlorobenzene NPW 1,4 Dichlorobenzene NPW Ethylbenzene NPW Hexachlorobutadiene NPW Naphthalene NPW Toluene NPW 1,2,4-Trichlorobenzene NPW Xylenes, total Volatile Halocarbons NPW Bromodichloromethane NPW Bromoform NPW Bromomethane NPW Carbon tetrachloride NPW Chlorobenzene NPW Chloroethane NPW Chloroform NPW Chloromethane NPW Dibromochloromethane NPW 1,2 Dichloroethane NPW 1,1-Dichloroethene NPW trans-1,2-Dichloroethene NPW 1,2-Dichloropropane NPW trans-1,3-Dichloropropene NPW Methylene Chloride NPW 4-Methyl-2-pentanone (MIBK) NPW Styrene NPW 1,1,2,2-Tetrachloroethane NPW Tetrachloroethene NPW 1,1,1-Trichloroethane NPW 1,1,2-Trichloroethane NPW Trichloroethene NPW Trichlorofluoromethane NPW Vinyl chloride Base/Neutrals NPW Acenaphthene NPW Acenaphthylene NPW Anthracene NPW Benzidine NPW Benzo(a)anthracene NPW Benzo(b)fluoranthene NPW Benzo(k)fluoranthene NPW Benzo(g,h,i)perylene NPW Benzo(a)pyrene NPW Benzylbutyl phthalate NPW 4-Bromophenyl-phenylether NPW bis(2-Chloroethoxy)methane NPW bis(2-Chloroethyl)ether NPW bis(2-Chloroisopropyl) ether NPW Bis(2-ethylhexyl) phthalate NPW 4-Chlorophenyl-phenylether NPW 2-Chloronaphthalene NPW Chrysene NPW Dibenzo(a,h)anthracene NPW Dibenzofuran NPW 1,2-Dichlorobenzene2 NPW 1,3-Dichlorobenzene2 NPW 1,4-Dichlorobenzene2 NPW 3,3`-Dichlorobenzidine NPW Diethyl phthalate NPW Dimethyl phthalate NPW Di-n-butylphthalate NPW 2,4-Dinitrotoluene NPW 2,6-Dinitrotoluene NPW Di-n-octylphthalate NPW Fluoranthene NPW Fluorene NPW Hexachlorobenzene NPW Hexachlorobutadiene2 NPW Hexachlorocyclopentadiene NPW Hexachloroethane NPW Indeno(1,2,3, cd)pyrene NPW Isophorone NPW 2-Methylnaphthalene NPW Naphthalene2 NPW Nitrobenzene NPW N-Nitrosodimethylamine NPW N-Nitroso-di-n-propylamine NPW N-Nitrosodiphenylamine NPW Phenanthrene NPW Pyrene NPW 1,2,4-Trichlorobenzene2 Acids NPW 4-Chloro-3-methylphenol NPW 2-Chlorophenol NPW 2,4-Dichlorophenol NPW 2,4-Dimethylphenol NPW 2,4-Dinitrophenol NPW 2-Methyl-4,6-Dinitrophenol NPW 2-Methylphenol (o-Cresol) NPW 4-Methylphenol (p-Cresol)3 NPW 2-Nitrophenol NPW 4-Nitrophenol NPW Phenol NPW Pentachlorophenol NPW 2,4,5-Trichlorophenol NPW 2,4,6-Trichlorophenol PCBs in Water NPW Aroclor 1016 NPW Aroclor 1221 NPW Aroclor 1232 NPW Aroclor 1242 NPW Aroclor 1248 NPW Aroclor 1254 NPW Aroclor 1260 Herbicides NPW 2,4-D NPW Dicamba NPW 2,4,5-T NPW 2,4,5-TP (Silvex) Radiochemistry4 Drinking Water/NPW Gross Alpha Drinking Water/NPW Gross Beta Drinking Water/NPW Radium 226 Drinking Water/NPW Radium 228 Drinking Water/NPW Uranium (Natural) Drinking Water/NPW Strontium 89 Drinking Water/NPW Strontium 90 Drinking Water/NPW Tritium Drinking Water/NPW Idodine 131 Drinking Water/NPW Barium 133 Drinking Water/NPW Cesium 134 Drinking Water/NPW Cesium 137 Drinking Water/NPW Cobalt 60 Drinking Water/NPW Zinc 65 1 Total Petroleum Hydrocarbons per solvent extraction with silica gel cleanup followed by gravimetric or infrared spectrometric technologies.
2 Dichlorobenzenes per solvent extraction and semivolatile analytical technologies.
3 Laboratories seeking or maintaining accreditation for Nonpotable Water 4-Methylphenol or the coeluting isomer pair of 3-Methylphenol and 4-Methylphenol must meet the PT requirements for this Field of Proficiency Testing (4-Methylphenol).
4 The PT study samples available for the Radio- chemistry group are acceptable for both Drinking Water and Nonpotable Water matrices.
Pennsylvania State (Chapter 252) Accreditation
Fields of Proficiency Testing
Drinking Water
Effective January 28, 2006
Matrix Analyte Microbiology Drinking Water Total Coliform Drinking Water Fecal Coliform/E.Coli Drinking Water Heterotrophic Plate Count Trace Metals Drinking Water Aluminum Drinking Water Antimony Drinking Water Arsenic Drinking Water Barium Drinking Water Beryllium Drinking Water Boron Drinking Water Cadmium Drinking Water Calcium Drinking Water Chromium Drinking Water Copper Drinking Water Iron Drinking Water Lead Drinking Water Magnesium Drinking Water Manganese Drinking Water Mercury Drinking Water Molybdenum Drinking Water Nickel Drinking Water Potassium Drinking Water Selenium Drinking Water Silver Drinking Water Thallium Drinking Water Uranium (Natural mass) Drinking Water Vanadiun Drinking Water Zinc Inorganic Disinfection By-Products Drinking Water Bromate Drinking Water Bromide Drinking Water Chlorate Drinking Water Chlorite Misc. Analytes Drinking Water Alkalinity as CaCO3/L Drinking Water Asbestos Drinking Water Ca Hardness as CaCO3 Drinking Water Total Hardness as CaCO3 Drinking Water Cyanide Drinking Water pH Drinking Water Residual Free Chlorine Drinking Water Total Residual Chlorine Drinking Water Sodium Drinking Water Specific Conductance Drinking Water Sulfate Drinking Water Total Filterable Residue Drinking Water Total Organic Carbon Drinking Water Turbidity Minerals Drinking Water Chloride Drinking Water Fluoride Drinking Water Nitrate as N Drinking Water Nitrite as N Drinking Water Nitrate + Nitrite as N Drinking Water Ortho-Phosphate Regulated VOCs Drinking Water Benzene Drinking Water Carbon Tetrachloride Drinking Water Chlorobenzene Drinking Water 1,2-Dichlorobenzene Drinking Water 1,4-Dichlorobenzene Drinking Water 1,2-Dichloroethane Drinking Water 1,1-Dichloroethylene Drinking Water Cis-1,2-Dichloroethylene Drinking Water Trans-1,2-Dichloroethylene Drinking Water Dichloromethane (Methylene Chloride) Drinking Water 1,2 Dichloropropane Drinking Water Ethylbenzene Drinking Water Styrene Drinking Water Tetrachloroethylene Drinking Water Toluene Drinking Water 1,1,1-Trichloroethane Drinking Water 1,1,2-Trichloroethane Drinking Water Trichloroethylene Drinking Water 1,2,4-Trichlorobenzene Drinking Water Vinyl Chloride Drinking Water Total Xylenes VOCs Drinking Water Bromobenzene Drinking Water Bromochloromethane Drinking Water Bromomethane Drinking Water n-Butylbenzene Drinking Water Sec-Butylbenzene Drinking Water Tert-Butylbenzene Drinking Water Chloroethane Drinking Water Chloromethane Drinking Water 2-Chlorotoluene Drinking Water 4-Chlorotoluene Drinking Water 1,2-Dibromo-3-chloropropane (DBCP) Drinking Water Dibromomethane Drinking Water 1,3-Dichlorobenzene Drinking Water Dichlorodifluoromethane Drinking Water 1,1-Dichloroethane Drinking Water 1,3-Dichloropropane Drinking Water 2,2-Dichloropropane Drinking Water 1,1-Dichloropropene Drinking Water Cis-1,3-Dichloropropene Drinking Water Trans-1,3-Dichloropropene Drinking Water Ethylene Dibromide (EDB) Drinking Water Hexachlorobutadiene Drinking Water Isopropylbenzene Drinking Water 4-Isopropyltoluene Drinking Water Methyl-tert-butylether (MTBE) Drinking Water n-Propylbenzene Drinking Water 1,1,1,2-Tetrachloroethane Drinking Water 1,1,2,2-Tetrachloroethane Drinking Water 1,2,3-Trichlorobenzene Drinking Water Trichlorofluoromethane Drinking Water 1,2,3-Trichloropropane Drinking Water 1,2,4-Trimethylbenzene Drinking Water 1,3,5-Trimethylbenzene Pesticides Drinking Water Alachlor Drinking Water Aldrin Drinking Water Atrazine Drinking Water Butachlor Drinking Water Chlordane (technical) Drinking Water Dieldrin Drinking Water Endrin Drinking Water Heptachlor Drinking Water Heptachlor Epoxide (beta) Drinking Water Hexachlorobenzene Drinking Water Hexachlorocyclopentadiene Drinking Water Lindane Drinking Water Methoxychlor Drinking Water Metolachlor Drinking Water Metribuzin Drinking Water Propachlor Drinking Water Simazine Drinking Water Toxaphene (total) Drinking Water Trifluralin Herbicides Drinking Water Acifluorfen Drinking Water 2,4-D Drinking Water 2,4-DB Drinking Water Dalapon Drinking Water Dicamba Drinking Water Dinoseb Drinking Water Diquat Drinking Water Endothall Drinking Water Glyphosate Drinking Water Pentachlorophenol Drinking Water Picloram Drinking Water 2,4,5-TP (Silvex) Drinking Water 2,4,5-T Organic Disinfection By-Products Drinking Water Chloral Hydrate Haloacetic acids Drinking Water Bromochloroacetic Acid Drinking Water Dibromoacetic Acid Drinking Water Dichloroacetic Acid Drinking Water Monobromoacetic Acid Drinking Water Monochloroacetic Acid Drinking Water Trichloroacetic Acid Trihalomethanes Drinking Water Bromodichloromethane Drinking Water Bromoform Drinking Water Chlorodibromomethane Drinking Water Chloroform Drinking Water Total Triholamethanes Adipate/Phthalate Drinking Water Di(2-Ethylhexyl) Adipate Drinking Water Di(2-Ethylhexyl) Phthalate PCBs in Water Drinking Water PCBs as decachlorobiphenyl Drinking Water PCB Aroclor Identification PAH Drinking Water Benzo(a)pyrene Carbamates and Vidate Drinking Water Aldicarb Drinking Water Aldicarb Sulfone Drinking Water Aldicarb Sulfoxide Drinking Water Carbaryl Drinking Water Carbofuran Drinking Water 3-Hydroxycarbofuran Drinking Water Methomyl Drinking Water Oxamyl (Vydate) Dioxin Drinking Water 2,3,7,8-Tetrachloro-dibenzodioxin Radiochemistry1 Drinking Water/NPW Gross Alpha Drinking Water/NPW Gross Beta Drinking Water/NPW Radium 226 Drinking Water/NPW Radium 228 Drinking Water/NPW Uranium (Natural) Drinking Water/NPW Strontium 89 Drinking Water/NPW Strontium 90 Drinking Water/NPW Tritium Drinking Water/NPW Idodine 131 Drinking Water/NPW Barium 133 Drinking Water/NPW Cesium 134 Drinking Water/NPW Cesium 137 Drinking Water/NPW Cobalt 60 Drinking Water/NPW Zinc 65 1 The PT study samples available for the Radiochem- istry group are acceptable for both Drinking Water and Nonpotable Water matrices.
Pennsylvania State (Chapter 252) Accreditation
Fields of Proficiency Testing
Solid and Chemical Materials (SCM)
Effective January 28, 2006
Matrix Analyte Metals Solid Aluminum Solid Antimony Solid Arsenic Solid Barium Solid Beryllium Solid Boron Solid Cadmium Solid Calcium Solid Chromium Solid Chromium VI Solid Cobalt Solid Copper Solid Iron Solid Lead Solid Magnesium Solid Manganese Solid Mercury Solid Molybdenum Solid Nickel Solid Potassium Solid Selenium Solid Silver Solid Sodium Solid Thallium Solid Tin Solid Vanadium Solid Zinc Inorganics Solid Cyanide Volatile Organics Solid Benzene Solid Bromodichloromethane Solid Bromoform Solid Carbon tetrachloride Solid Chlorobenzene Solid Chlorodibromomethane Solid Chloroform Solid 1,2 Dichlorobenzene Solid 1,3 Dichlorobenzene Solid 1,4 Dichlorobenzene Solid 1,1 Dichloroethane Solid 1,2 Dichloroethane Solid Ethylbenzene Solid Methylene Chloride Solid 4-Methyl-2-pentanone (MIBK) Solid 1,1,1,2-Tetrachloroethane Solid 1,1,2,2-Tetrachloroethane Solid Tetrachloroethene Solid Toluene Solid 1,1,1-Trichloroethane Solid Trichloroethene Solid Xylenes, total BNA Solid Acenaphthene Solid Acenaphthylene Solid Anthracene Solid Benzo(a)anthracene Solid Benzo(a)pyrene Solid Benzo(b)fluoranthene Solid Benzo(g,h,i)perylene Solid Benzo(k)fluoranthene Solid bis(2-Chloroisopropyl) ether Solid bis(2-Chloroethoxy)methane Solid Bis(2-ethylhexyl) phthalate Solid 4-Bromophenyl-phenylether Solid Butylbenzylphthalate Solid 2-Chlorophenol Solid 4-Chloro-3-methylphenol Solid 2-Chloronaphthalene Solid 4-Chlorophenyl-phenylether Solid Chrysene Solid Dibenzo(a,h)anthracene Solid Dibenzofuran Solid 2,4-Dichlorophenol Solid Diethyl phthalate Solid Dimethyl phthalate Solid Di-n-butylphthalate Solid 2,4-Dimethylphenol Solid 2,4-Dinitrophenol Solid 2,4-Dinitrotoluene Solid 2,6-Dinitrotoluene Solid Di-n-octylphthalate Solid Fluoranthene Solid Fluorene Solid Hexachlorobenzene Solid Hexachlorobutadiene Solid Hexachlorocyclopentadiene Solid Hexachloroethane Solid Indeno(1,2,3,-cd)pyrene Solid Isophorone Solid 2-Methyl-4,6-Dinitrophenol Solid 2-Methylphenol Solid Naphthalene Solid Nitrobenzene Solid N-Nitroso-di-n-propylamine Solid 2-Nitrophenol Solid 4-Nitrophenol Solid Pentachlorophenol Solid Phenanthrene Solid Phenol Solid Pyrene Solid 1,2,4-Trichlorobenzene Solid 2,4,5-Trichlorophenol Solid 2,4,6-Trichlorophenol PCBs Solid Aroclor 1016 Solid Aroclor 1221 Solid Aroclor 1232 Solid Aroclor 1242 Solid Aroclor 1248 Solid Aroclor 1254 Solid Aroclor 1260 PCBs in Oil Oil Aroclor 1016/1242 Oil Aroclor 1254 Oil Aroclor 1260 Pesticides Solid Aldrin Solid alpha-BHC Solid beta-BHC Solid delta-BHC Solid gamma-BHC (Lindane) Solid Chlordane Solid 4,4`-DDD Solid 4,4`-DDE Solid 4,4`-DDT Solid Dieldrin Solid Endosulfan I Solid Endosulfan II Solid Endosulfan sulfate Solid Endrin Solid Endrin aldehyde Solid Heptachlor Solid Heptachlor Epoxide Solid Methoxychlor Solid Toxaphene Herbicides Solid Dicamba Solid Disulfoton Solid 2,4-D Solid 2,4,5-T Solid 2,4,5-TP (Silvex)
[Pa.B. Doc. No. 06-397. Filed for public inspection March 10, 2006, 9:00 a.m.]
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